manuais Beverage-Air NC49

Beverage air NC49 Manual (67 páginas)

Marca: Beverage-air | Categoria: não | Tamanho: 2.31 MB |

Inglês

Índice

AminoPac

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AAA-Direct

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©Dionex Corporation, 2006

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Document No. 031481

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Revision 12

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November 2006

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TABLE OF CONTENTS

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SECTION 1 - INTRODUCTION

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2.1 System Requirements

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3.1 Deionized Water

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3.2 Sodium Hydroxide

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3.3 Sodium Acetate

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SECTION 4 - GETTING STARTED

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4.2 Initial Check List

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5.5 Amino Acid Standards

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6.1.2 Software Installation

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6.1.3 System Rinse

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6.2.1 System Background Check

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Ca. 30 nC

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6.4.2 Column Installation

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6.4.3 Histidine Injection

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Overlay of lines 3 and 4

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Peak height ~150 nC

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6.6 System Shutdown

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Figure 5

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Overview of Gradient Methods

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SECTION 8 - APPLICATIONS

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HCl Hydrolysate

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M Standard

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8.3 Analysis of Tryptophan

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Standard

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Performic Acid/HCl

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Hydrolysate

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0 5.00 10.00 15.00 20.00

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Carrot Juice

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Figure 16B

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Figure 16A

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8.10 AAA Recommended Reading

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Eluent 1: 10 mM NaOH

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Eluent 2: 250 mM NaOH

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Gradient Conditions for

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above gradient table

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SECTION 10 - TROUBLESHOOTING

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10.3 Column Problems

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10.4 System Problems

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Oxygen Dip

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10.5 Sodium Hydroxide Cleanup

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10.6 Nitric Acid Cleanup

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10.7 Acetate Line Cleanup

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10.8.1 Mechanical Polishing

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Reference Electrode

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Cylinder

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Thumbscrew

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Cell Cover

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Cell Body

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J2 Connector

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Junction

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APPENDIX A - COLUMN CARE

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